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  • Gravimetric Analysis

    The ion being analyzed must be completely precipitated. The precipitate must be a pure compound. The precipitate must be easily filtered. An example of a gravimetric analysis is the determination of chloride in a compound. In order to do a gravimetric analysis, a ion must be found that forms an insoluble compound with chloride. This compound must also be pure and easily filtered. The ...

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  • : Precipitation Gravimetry

    Theory and Practice. All precipitation gravimetric analysis share two important attributes. First, the precipitate must be of low solubility, of high purity, and of known composition if its mass is to accurately reflect the analyte's mass. Second, the precipitate must be easy to separate from the reaction mixture.

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  • Experiment 2

    The precipitation of the nickel occurs by complexation of the Ni2+ ion forming the Ni(dmg) 2 complex which is almost insoluble in water. C C O O H 3 C H 3 C CH 3. Biacetyl + 2 NH 2 OH. Hydroxylamine. C C CH 3 + 2 H 2 O. Dimethylglyoxime. HON NOH. The precipitating agent dimethylglyoximate (dmg) is virtually specific reagent for Ni. Pd2+ likewise forms a precipitate .

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  • Chapter 1

    4 Analytical Chemistry The development, in 1905, of dimethylglyoxime (dmg), a reagent that selectively precipitates Ni2+ and Pd2+, led to an improved analytical method for the quantitative analysis of The resulting analysis, as shown in Figure .

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  • Nickel: Chemical reactions | Pilgaard Elements

    Nickel metal dissolves slowly in dilute sulphuric acid to form the aquated Ni(II) ion and hydrogen, H aqueous solution, Ni(II) is present as the complex ion [Ni(H 2 O) 6] 2+. Ni (s) + H 2 SO 4 (aq) Ni 2+ (aq) + SO 4 2− (aq) + H 2 (g) The strongly oxidizing concentrated nitric acid, HNO 3, reacts on the surface of iron and passivates the surface.

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